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Structure of N-[bis(methylthio)methylene]cinnamamide, C12H13NOS2

Kamath, NU and Venkatesan, K (1984) Structure of N-[bis(methylthio)methylene]cinnamamide, C12H13NOS2. In: Acta crystallographica section c-crystal structure communications, 40 (9). pp. 1610-1612.

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Abstract

M r = 251.34, monoclinic, P21/n, a =14.626 (3), b= 7.144 (1), c= 11.996 (2)\AA \betat=90.03 (2) °, V= 1253.4 (6) \AA 3, Z = 4, Dm= 1.326 (3),Dx=1.331(3)gcm -3, MoKat, \lambda = 0.7107 )\AA , \mu=3.51 cm -3, F(000) = 528.0, T-- 293 K, R -- 3.5% for1455 significant reflections. Of particular interest is an intramolecular attractive interaction between the sulphur and oxygen atoms with an S...O distance of 2.658 (3)\AA, in which the oxygen atom appears to actas a nucleophile.

Item Type: Journal Article
Additional Information: Copyright for this article belongs to International Union of Crystallography.
Department/Centre: Division of Chemical Sciences > Organic Chemistry
Date Deposited: 04 Feb 2010 07:03
Last Modified: 19 Sep 2010 05:34
URI: http://eprints.iisc.ernet.in/id/eprint/20721

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