Vanishri, S and Marin, C and Bhat, HL and Salce, B and Braithwaite, D and Regnault, LP (2009) Crystal growth and characterization of two-leg spin ladder compounds: Sr14Cu24O41 and Sr2Ca12Cu24O41. In: Journal of Crystal Growth, 311 (15). pp. 3830-3834.
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Single crystals of Sr14−xCaxCu24O41 (x=0 and 12) are grown by the travelling solvent floating zone technique using an image furnace. The grown crystals are characterized for their single crystallinity by the X-ray and Neutron Laue method. The magnetic susceptibility measurements in Sr14Cu24O41 show considerable anisotropy along the main crystallographic axes. Low-temperature specific heat measurement and DC susceptibility measurement in Ca-doped crystal showed antiferromagnetic ordering at 2.8 K at ambient pressure. High-pressure AC susceptibility measurement on Ca-doped crystal showed a sharp superconducting transition at 2 K under 40 kbars. Tc onset reached a maximum value of 9.9 K at 54 kbars. The bulk superconductivity of the sample is confirmed by the high-pressure AC calorimetry with Tc max=9.4 K and TN=5 K at 56 kbars.
|Item Type:||Journal Article|
|Additional Information:||Copyright of this article belongs to Elsevier Science.|
|Keywords:||Floating zone technique;Single crystal growth;Travelling solvent zone growth;Cuprates;Oxide superconducting materials.|
|Department/Centre:||Division of Physical & Mathematical Sciences > Physics|
|Date Deposited:||27 Oct 2009 12:22|
|Last Modified:||19 Sep 2010 05:45|
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