Ramakumar, Suryanarayanarao and Venkatesan, K and Rao, ST (1977) The Crystal and Molecular Structure of l-(Diphenylmethyl)azetidin-3-ol. In: Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry, 33 (3). pp. 824-829.
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1-(Diphenylmethyl)azetidin-3-ol is triclinic, space group P1, with a=8.479(2), b=17.294(4),c = 10.606 (3) A, a = 118.59 (2),/~ = 100.30 (2), y = 89.63 (2) °, Z = 4. The structure was solved by multisolution methods and refined to an R of 0.044 for 2755 reflexions. The four-membered rings in the two independent molecules are puckered with dihedral angles of 156 and 153 ° . The two molecules differ in conformation with respect to rotation of the phenyl rings about the C-C bonds. The structure is stabilized by a network of O-H. • • N intermolecular hydrogen bonds.
|Item Type:||Journal Article|
|Additional Information:||Copyright of this article belongs to International Union of Crystallography.|
|Department/Centre:||Division of Chemical Sciences > Organic Chemistry|
|Date Deposited:||01 Feb 2010 06:09|
|Last Modified:||19 Sep 2010 05:51|
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