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The Crystal and Molecular Structure of l-(Diphenylmethyl)azetidin-3-ol

Ramakumar, Suryanarayanarao and Venkatesan, K and Rao, ST (1977) The Crystal and Molecular Structure of l-(Diphenylmethyl)azetidin-3-ol. In: Acta Crystallographica Section B Structural Crystallography and Crystal Chemistry, 33 (3). pp. 824-829.

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Official URL: http://scripts.iucr.org/cgi-bin/paper?a14504

Abstract

1-(Diphenylmethyl)azetidin-3-ol is triclinic, space group P1, with a=8.479(2), b=17.294(4),c = 10.606 (3) A, a = 118.59 (2),/~ = 100.30 (2), y = 89.63 (2) °, Z = 4. The structure was solved by multisolution methods and refined to an R of 0.044 for 2755 reflexions. The four-membered rings in the two independent molecules are puckered with dihedral angles of 156 and 153 ° . The two molecules differ in conformation with respect to rotation of the phenyl rings about the C-C bonds. The structure is stabilized by a network of O-H. • • N intermolecular hydrogen bonds.

Item Type: Journal Article
Additional Information: Copyright of this article belongs to International Union of Crystallography.
Department/Centre: Division of Chemical Sciences > Organic Chemistry
Date Deposited: 01 Feb 2010 06:09
Last Modified: 19 Sep 2010 05:51
URI: http://eprints.iisc.ernet.in/id/eprint/24614

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