Dix, Ina and Hopf, Henning and Satyanarayana, Thota BN and Ernst, Ludger (2010) Preparation and NMR spectra of four isomeric diformyl2.2]paracyclophanes (cyclophanes 66). In: Beilstein Journal of Organic Chemistry, 6 . pp. 932-937.
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Four isomeric dialdehydes 4, readily available from cycloaddition of propiolic aldehyde (2) to 1,2,4,5-hexatetraene (1), were separated by chromatography and recrystallization, and were characterized by their spectroscopic data. The individual isomers can now be easily identified from their H-1 NMR spectra even if only one of them is present.
|Item Type:||Journal Article|
|Additional Information:||Copyright of this article belongs to BioMed Central.|
|Keywords:||cyclophanes; diformyl2.2]paracyclophanes; layered compounds; NMR spectroscopy; structure assignment|
|Department/Centre:||Division of Chemical Sciences > Organic Chemistry|
|Date Deposited:||19 Nov 2010 11:11|
|Last Modified:||19 Nov 2010 11:11|
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